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HRID735985

反应详情

EQUATION

反应方程式

HRID 735985 的结构方程式

REACTANTS

反应物

2
结构：CCCCCCc1ccc(C#Cc2ccc(C=O)cc2)cc1
HCID11289286

未命名化合物

结构：CC(C)(N)c1cccc(Cl)c1
HCID13569521

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCc1ccc(C#Cc2ccc(CNC(C)(C)c3cccc(Cl)c3)cc2)cc1
HCID67187575

未命名化合物

收率 80%

PROCEDURE

实验过程

The same procedure as employed in the preparation of Example 226 (step a) but using 4-[(4-hexylphenyl)ethynyl]benzaldehyde and 1-(3-chlorophenyl)-1-methylethylamine gave the title compound as a brown oil (80%). HPLC (Condition A), Rt: 4.73 min (HPLC purity: 98.7%).

WORKUP

后处理

  1. customThe same procedure as employed in the preparation of Example 226 (step a) but