HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-[(4-Hexylphenyl)ethynyl]benzaldehyde → N-[1-(3-chlorophenyl)-1-methylethyl]-N-{4-[(4-hexylphenyl)-ethynyl]benzyl}amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-[(4-Hexylphenyl)ethynyl]benzaldehyde | HCID 11289286 | — |
| Reactant | 2-(3-Chlorophenyl)propan-2-amine | HCID 13569521 | — |
| Product | N-[1-(3-chlorophenyl)-1-methylethyl]-N-{4-[(4-hexylphenyl)-ethynyl]benzyl}amine | HCID 67187575 | 80% |
Reaction Steps
The same procedure as employed in the preparation of Example 226 (step a) but using 4-[(4-hexylphenyl)ethynyl]benzaldehyde and 1-(3-chlorophenyl)-1-methylethylamine gave the title compound as a brown oil (80%). HPLC (Condition A), Rt: 4.73 min (HPLC purity: 98.7%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592477B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-79386f64b5484cb4b5ccf6e39f4839cc |
| Source note | uspto-grants-2009_09 |