HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Fluorophenyl)ethylamine → N-(4-dodec-1-ynylbenzyl)-N-[2-(2-fluorophenyl)ethyl]amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Fluorophenyl)ethylamine | HCID 643357 | — |
| Reactant | 4-Dodec-1-ynylbenzaldehyde | HCID 86598536 | — |
| Product | N-(4-dodec-1-ynylbenzyl)-N-[2-(2-fluorophenyl)ethyl]amine | HCID 67187042 | — |
Reaction Steps
The same procedure as employed in the preparation of Example 394 (step b) but using 4-dodec-1-ynylbenzaldehyde and 2-(2-fluorophenyl)ethylamine gave the title compound as an oil. M+(LC/MS(ESI)): 394.4. HPLC (Condition A), Rt: 5.00 min (HPLC purity: 93.6%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592477B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-b8c52715351c4a4995ed7a069fc7149e |
| Source note | uspto-grants-2009_09 |