HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Trifluoromethyl)benzylamine → HCID 67186742, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Trifluoromethyl)benzylamine | HCID 76447 | — |
| Reactant | 4-Dec-1-ynylbenzaldehyde | HCID 57841320 | — |
| Product | HCID 67186742 | HCID 67186742 | — |
Reaction Steps
The same procedure as employed in the preparation of Example 394 (step b) but using 4-dec-1-ynylbenzaldehyde and 2-(trifluoromethyl)benzylamine gave the title compound as an oil. M+(LC/MS(ESI)): 402.3. HPLC (Condition A), Rt: 4.71 min (HPLC purity: 86.5%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592477B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-8019d8244b5d45c0bbed163aa6bb5988 |
| Source note | uspto-grants-2009_09 |