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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 736011Generated: October 30, 2026

HCID 57847747, compound → HCID 69472192, compound

https://huagongshe.com/reaction/736011

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 57847747HCID 57847747—
SolventTetrahydrofuranHCID 8028—
ProductHCID 69472192HCID 69472192—

Reaction Steps

A solution of 4-(5-tert-butyl-2-phenyl-3-furyl)pyridin-2(1H)-one (50 mg, 0.2 mmol) in THF (50 mL) was irradiated with a sun lamp for 5 h. The solution was then concentrated in vacuo and the product purified by flash chromatography using EtOAc-Pet. Spirit (80:20) as eluant, to separate the pure product as a cream solid (26 mg, 52%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07593820B2
Source datasetuspto-grants-2009_09
ORD IDord-c2f57943da1a40f8875d5c0d20ca8946
Source noteuspto-grants-2009_09