HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57847747, compound → HCID 69472192, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57847747 | HCID 57847747 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 69472192 | HCID 69472192 | — |
Reaction Steps
A solution of 4-(5-tert-butyl-2-phenyl-3-furyl)pyridin-2(1H)-one (50 mg, 0.2 mmol) in THF (50 mL) was irradiated with a sun lamp for 5 h. The solution was then concentrated in vacuo and the product purified by flash chromatography using EtOAc-Pet. Spirit (80:20) as eluant, to separate the pure product as a cream solid (26 mg, 52%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07593820B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-c2f57943da1a40f8875d5c0d20ca8946 |
| Source note | uspto-grants-2009_09 |