HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → 2-Chloro-5-(ethylsulfamoyl)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | Benzoic acid, 2-chloro-5-[(methylamino)sulfonyl]- | HCID 111724 | — |
| Reactant | 2-Chloro-5-sulfino-benzoic acid | HCID 15112904 | — |
| Product | 2-Chloro-5-(ethylsulfamoyl)benzoic acid | HCID 16768323 | 78% |
Reaction Steps
The title compound was synthesised according to the procedure described for 2-Chloro-5-methylsulfamoyl-benzoic acid from 2-Chloro-5-sulfino-benzoic acid and ethylamine and obtained in 78% yield. MS (m/e): 262.2 (MH−, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07595314B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-c1f91aa6c40c45dd80d4157aa6073ca8 |
| Source note | uspto-grants-2009_09 |