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HRID736347

反应详情

EQUATION

反应方程式

HRID 736347 的结构方程式

REACTANTS

反应物

3
结构：CON(C)C(=O)c1ccnc(Cl)c1
HCID18506894

2-Chloro-N-methoxy-N-methyl-4-pyridinecarboxamide

C8H9ClN2O2

结构：CC(C)n1cc(Br)c2c(Cl)ncnc21
HCID45789428

5-Bromo-4-chloro-7-(propan-2-yl)-7H-pyrrolo[2,3-d]pyrimidine

C9H9BrClN3

结构：CC(C)n1cc(C(=O)c2cncc(Br)c2)c2c(Cl)ncnc21
HCID86603152

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)n1cc(C(=O)c2ccnc(Cl)c2)c2c(Cl)ncnc21
HCID86603156

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 5-Bromo-4-chloro-7-isopropyl-7H-pyrrolo[2,3-d]pyrimidine (6.5 g, 23.7 mmol) and 2-Chloro-N-methoxy-N-methyl-isonicotinamide (5.7 g, 28.4 mmol) by procedures analogous to those described for the preparation of (5-Bromo-pyridin-3-yl)-(4-chloro-7-isopropyl-7H-pyrrolo[2,3-d]pyrimidin-5-yl)-methanone. MS: 295.8 (MH−); HPLC Rf: 2.0 min. (HPLC method 2); HPLC purity: 100%.