(phenylsulfonyl)acetic acid → HCID 9949099, compound

HRID 736534Notes

Reaction equation

HRID 736534 reaction equation
[C:1]1([S:7]([CH2:10][C:11](O)=O)(=[O:9])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Br:14][C:15]1[CH:22]=[CH:21][C:18](C=O)=[CH:17][CH:16]=1>>[C:1]1([S:7](/[CH:10]=[CH:11]/[C:18]2[CH:21]=[CH:22][C:15]([Br:14])=[CH:16][CH:17]=2)(=[O:9])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 59543(phenylsulfonyl)acetic acidHCID 707414-Bromobenzaldehyde

Product 1

HCID 9949099HCID 9949099, compoundYield 78%

Procedure

A solution of phenyl sulfonylacetic acid (0.01 mol) and 4-bromobenzaldehyde (0.01 mol) was subjected to Procedure 1, Part B. The title compound was obtained in 78-80% yield.

Sources & evidence

ORD record
ord-b45e2485993842dd98cb0c50b51d5461
Source dataset
uspto-grants-2009_09
Patent number
US07595347B2

Reaction notes

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