4-Chlorobenzaldehyde → HCID 9839787, compound

HRID 736535Notes

Reaction equation

[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([CH2:11][C:12](O)=O)(=[O:10])=[O:9])=[CH:4][CH:3]=1.[Cl:15][C:16]1[CH:23]=[CH:22][C:19](C=O)=[CH:18][CH:17]=1>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8](/[CH:11]=[CH:12]/[C:19]2[CH:22]=[CH:23][C:16]([Cl:15])=[CH:17][CH:18]=2)(=[O:10])=[O:9])=[CH:4][CH:3]=1

Participants

Reactant 2

HCID 77264-Chlorobenzaldehyde

HCID 55680(4-Chlorobenzene-1-sulfonyl)acetic acid

Product 1

HCID 9839787HCID 9839787, compoundYield 70%

Procedure

A solution of 4-chlorophenyl sulfonylacetic acid (0.01 mol) and 4-chlorobenzaldehyde (0.01 mol) was subjected to Procedure 1, Part B. The title compound was obtained in 70-72% yield.

Sources & evidence

ORD record: ord-25cd4632aa914837aec9e14912059963
Source dataset: uspto-grants-2009_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07595347B2

Reaction notes

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