HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Bromide → HCID 67291218, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Bromide | HCID 6332 | — |
| Reactant | HCID 57849395 | HCID 57849395 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 67291218 | HCID 67291218 | — |
Reaction Steps
Ethylbromide (12 ml) is added to a solution of 2-(2,6-diethyl-4-hydroxy-2,3,6-trimethyl-piperidine-1-yloxy)-N-(3-dimethylamino-propyl)-2-methyl-propionamide (20.5 g, 0.053 mol, compound 110) in acetonitrile (35 ml). The mixture is stirred for 18 h at room temperature and is then evaporated to afford 26.63 g of the title compound as a colorless solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07595359B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-7d0f311d024f4991b83fe0a6cfeb8b9a |
| Source note | uspto-grants-2009_09 |