Bis(2-Methoxyethyl)amine → HCID 10450631, compound

HRID 736609Notes

Reaction equation

HRID 736609 reaction equation
[CH3:1][O:2][CH2:3][CH2:4][NH:5][CH2:6][CH2:7][O:8][CH3:9].[Br:10][C:11]1[CH:16]=[CH:15][C:14]([S:17](Cl)(=[O:19])=[O:18])=[CH:13][CH:12]=1>>[Br:10][C:11]1[CH:16]=[CH:15][C:14]([S:17]([N:5]([CH2:6][CH2:7][O:8][CH3:9])[CH2:4][CH2:3][O:2][CH3:1])(=[O:19])=[O:18])=[CH:13][CH:12]=1

Participants

3

Reactant 2

HCID 2383Bis(2-Methoxyethyl)amineHCID 7396p-Bromobenzenesulfonyl chloride

Product 1

HCID 10450631HCID 10450631, compoundYield 99%

Procedure

Starting materials: bis(2-methoxyethyl)amine and 4-bromobenzenesulfonyl chloride. Yield: 99% as a yellow oil: 1H NMR (CDCl3) δ 7.69 (d, J=9 Hz, 2H), δ 7.62 (d, J=9 Hz, 2H), 3.49 (m, 4H), 3.39 (m, 4H), 3.27 (s, 6H); MS (ESP) m/z 352, 354 (M++1).

Sources & evidence

ORD record
ord-f4eacb4fcfef44dd8f935744faec264c
Source dataset
uspto-grants-2009_09
Patent number
US07595319B2

Reaction notes

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