HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22184582, compound → 4-Amino-3-chloro-5-(trifluoromethyl)benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22184582 | HCID 22184582 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 4-Amino-3-chloro-5-(trifluoromethyl)benzaldehyde | HCID 13020473 | — |
Reaction Steps
A mixture of 17.0 g (75.4 mmol) of (4-amino-3-chloro-5-trifluoromethyl-phenyl)-methanol, 100 g (1.15 mol) of manganese dioxide and 300 mL of DCM was stirred overnight at RT. The precipitate was suction filtered and the solution evaporated down i. vac. The desired product was obtained as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07595312B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-a4d420529fd54807a75a58a761b9794f |
| Source note | uspto-grants-2009_09 |