HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 57849511, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Bromobenzyl bromide | HCID 68527 | — |
| Reactant | 2-Phenylpiperazine | HCID 250673 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 57849511 | HCID 57849511 | 55.4% |
Reaction Steps
1.54 g of 4-Bromobenzyl bromide and 1 g of 3-Phenylpiperazine in 20 mL of acetonitrile were stirred at room temperature and 0.85 g of potassium carbonate was added. The reaction was stirred at room temperature overnight. The solution was filtered through Celite and concentrated in vacuo. Purification was done by flash chromatography to afford 1.13 g of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07595397B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-fe3a2ff7118a402a97853f881a0d5527 |
| Source note | uspto-grants-2009_09 |