HRID737086

反应详情

EQUATION

反应方程式

HRID 737086 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

1.54 g of 4-Bromobenzyl bromide and 1 g of 3-Phenylpiperazine in 20 mL of acetonitrile were stirred at room temperature and 0.85 g of potassium carbonate was added. The reaction was stirred at room temperature overnight. The solution was filtered through Celite and concentrated in vacuo. Purification was done by flash chromatography to afford 1.13 g of product.

WORKUP

后处理

  1. filtrationThe solution was filtered through Celite
  2. concentrationconcentrated in vacuo
  3. customPurification