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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 737092Generated: October 30, 2026

Potassium Carbonate → HCID 57849544, compound

https://huagongshe.com/reaction/737092

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant4-Bromobenzyl bromideHCID 68527—
Reactant3-PhenylpyrrolidineHCID 3146743—
SolventAcetonitrileHCID 6342—
ProductHCID 57849544HCID 578495442%

Reaction Steps

5.632 g of 4-Bromobenzyl bromide and 2.211 of 3-Phenylpyrrolidine (Array) in 50 mL of acetonitrile were stirred at room temperature and 6.229 g of potassium carbonate was added. The reaction was stirred at room temperature overnight. The solution was filtered through Celite and concentrated in vacuo to afford a brown solid. Purification was done by flash chromatography to afford product. Wt: 33 mg, 2% yield, ES MS m/z 316/318

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07595397B2
Source datasetuspto-grants-2009_09
ORD IDord-efe8d99b972144ca8cadf9d5ac6c6bd6
Source noteuspto-grants-2009_09