HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 57849544, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Bromobenzyl bromide | HCID 68527 | — |
| Reactant | 3-Phenylpyrrolidine | HCID 3146743 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 57849544 | HCID 57849544 | 2% |
Reaction Steps
5.632 g of 4-Bromobenzyl bromide and 2.211 of 3-Phenylpyrrolidine (Array) in 50 mL of acetonitrile were stirred at room temperature and 6.229 g of potassium carbonate was added. The reaction was stirred at room temperature overnight. The solution was filtered through Celite and concentrated in vacuo to afford a brown solid. Purification was done by flash chromatography to afford product. Wt: 33 mg, 2% yield, ES MS m/z 316/318
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07595397B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-efe8d99b972144ca8cadf9d5ac6c6bd6 |
| Source note | uspto-grants-2009_09 |