HRID737104

反应详情

EQUATION

反应方程式

HRID 737104 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The above compound could be made in the following manner: 1.5 eq. of 4-Bromobenzyl bromide and 1 eq. of 2-Benzyl-morpholine in acetonitrile could be stirred at room temperature and 3 eq. of potassium carbonate could be added. The reaction could be stirred at room temperature overnight. The solution could be filtered through Celite and concentrated in vacuo to afford a brown solid. Purification could be done by flash chromatography to afford product.

WORKUP

后处理

  1. customThe reaction
  2. filtrationThe solution could be filtered through Celite
  3. concentrationconcentrated in vacuo
  4. customto afford a brown solid
  5. customPurification
  6. customto afford product