反应详情

温度

0 °C

80 mg (0.19 mmol)) of Compound 5050 was dissolved in 5 mL of dry methylene chloride. To this solution at 0° C. was added triethylamine (0.19 mmol, 25 μL) followed by pentanoyl chloride (0.19 mmol, 22 μL). Reaction mixture was stirred at 0° C. for 15 minutes. Reaction mixture was quenched using water and evaporated. It was redissolved in 5 mL of DMF and purified using reverse phase HPLC. MS: 507.2 (M+H+).

1. customReaction mixture
2. customReaction mixture
3. customwas quenched
4. customevaporated
5. dissolutionIt was redissolved in 5 mL of DMF
6. custompurified