HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → 5-acetyl-2-Furancarboxylic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | Methyl 5-(2-bromoacetyl)furan-2-carboxylate | HCID 14945157 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 5-acetyl-2-Furancarboxylic acid methyl ester | HCID 12281225 | — |
Reaction Steps
Bromination of 5-acetyl-furan-2-carboxylic acid methyl ester (0.27 g, 1.61 mmol) with Br2 (0.082 mL) in AcOH (6 mL) at room temperature gave 5-(2-bromo-acetyl)-furan-2-carboxylic acid methyl ester; MS: 246.1 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07595398B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-893a7dce008b4f8b82f1fe47f51916d8 |
| Source note | uspto-grants-2009_09 |