HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Acetate → HCID 86616441, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | Thiourea | HCID 2723790 | — |
| Reactant | HCID 86616442 | HCID 86616442 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86616441 | HCID 86616441 | — |
Reaction Steps
A mixture of 6-(2-bromo-acetyl)-nicotinic acid benzyl ester (0.16 g, 0.48 mmol), thiourea (0.0.038 g), and NaOAc (0.051 g) in EtOH (6 mL) was stirred at room temperature overnight. The mixture was concentrated in vacuo to give the crude product 6-(2-Amino-thiazol-4-yl)-nicotinic acid benzyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07595398B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-6bf6a643b04c4bd78ec1ebd23b6e84b6 |
| Source note | uspto-grants-2009_09 |