HRID737217

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID7813

4-Methylbenzenamine

C7H9N

HCID67993

lpha,alpha,alpha-Trifluoro-4-iodotoluene

C7H4F3I

PRODUCTS

生成物

HCID18712799

4-Methyl-N-[4-(trifluoromethyl)phenyl]aniline

C14H12F3N

收率 47.516%

AUXILIARIES

试剂、催化剂与溶剂

结构：CCN=P(N=P(N(C)C)(N(C)C)N(C)C)(N(C)C)N(C)C

试剂HCID3393106

Phosphazene base P2-Et

C12H35N7P2

结构：CC(C)c1cc(C(C)C)c(-c2ccccc2P(C2CCCCC2)(C2CCCCC2)->[Pd]2(<-Nc3ccccc3-c3ccccc32)OS(=O)(=O)C(F)(F)F)c(C(C)C)c1

催化剂HCID178439018

未命名化合物

溶剂HCID679

Dimethyl sulfoxide

C2H6OS

5 次

CONDITIONS

反应条件

温度: 60 °C

PROCEDURE

实验过程

These solutions were added to a 384- well source plate (80 µL per well). The Mosquito HTS liquid handling robot was used to dose each of these solutions (200 nL each) into a 1536-well plate.

WORKUP

后处理

addition未记录说明