HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 9-Borabicyclo[3.3.1]nonane, 9-chloro-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 9-Borabicyclo(3.3.1)nonane | HCID 78966 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | 9-Borabicyclo[3.3.1]nonane, 9-chloro- | HCID 10909822 | 75% |
Reaction Steps
The title compound was prepared in 75% yield following the method of Example 1 by treating 9-borabicyclo[3.3.1]nonane (9-BBN, Aldrich Chemical Company, Inc., Milwaukee, Wis.) with anhydrous HCl in ether. 11B NMR δ 79 ppm in hexane, bp 65° C. (0.3 mm).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05552081 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-9595334a782f420e929bf7c210e29da7 |
| Source note | uspto-grants-1996_09 |