Phenol → HCID 19426966, compound

HRID 741803Notes

Reaction equation

HRID 741803 reaction equation
[C:1]1([OH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C[Mg+].[Br-]>C1COCC1>[OH:7][C:1]([C:3]1[CH:2]=[C:1]([OH:7])[CH:6]=[CH:5][CH:4]=1)([CH2:6][CH3:5])[CH2:2][CH3:3]

Participants

4

Reactant 2

HCID 996Phenol2×HCID 178418689HCID 178418689, compound

Product 1

HCID 19426966HCID 19426966, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

Following the procedure described for Phenol 13, Step 2 and for Phenol 7, Step 3 but substituting EtMgBr in THF (Aldrich) for MeMgBr, the title compound was obtained.

Sources & evidence

ORD record
ord-c1f1c57576934826a6f35fd766ea1cd8
Source dataset
uspto-grants-1996_09
Patent number
US05552437

Reaction notes

Loading…