Triethylamine → HCID 19069747, compound

Participants

Reaction Steps

The title compound was prepared by the procedure described in Example 19 using 9.2 g of N-ethyl glycine, 5.7 g of isobutyl-isothiocyanate, 10.1 g of triethylamine, and 150 mL of methylene chloride. Purification was achieved by flash chromatography on silica gel (methylene chloride). Title compound (2.3 g) was obtained as an oil. Anal. Calcd. for. C9H16N2O S: C, 53.97; H, 8.05; N, 13.99. Found: C, 54.01; H, 8.21; N, 14.00) Mass spectrum (El, M.+) m/z 200.

Provenance & Evidence