Triethylamine → HCID 19425379, compound

Participants

Reaction Steps

The title compound was prepared by the; procedure described in Example 19 using 9.2 g of N-ethyl glycine, 8.48 g of 2-chlorophenyl-isothiocyanate, 10.1 g of triethylamine, and 150 mL of methylene chloride. Purification was achieved through crystallization from ethanol. Title compound (3.85 g) was obtained as an orange solid, m.p. 142°-145° C. Anal. Calcd. for. C11H11Cl N2O S: C, 51.87; H, 4.35; N, 11.00. Found: C, 51.96; H, 4.26; N, 10.97. Mass spectrum (EI, M.+) m/z 254.

Provenance & Evidence