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HRID742962

反应详情

EQUATION

反应方程式

HRID 742962 的结构方程式

REACTANTS

反应物

2
结构：ClCCl
HCID6344

Dichloromethane

CH2Cl2

结构：Cn1c(=O)[nH]c2c(c1=O)CN(Cc1ccccc1)CC2
HCID10016028

未命名化合物

PRODUCTS

生成物

1
结构：Cl.Cn1c(=O)[nH]c2c(c1=O)CN(Cc1ccccc1)CC2
HCID19423353

未命名化合物

PROCEDURE

实验过程

14.3 g of 6-benzyl-3-methyl-5,6,7,8-tetrahydro-1H-pyrido[4,3-d]pyrimidine-2,4-dione were dissolved in 300 ml of dichloromethane, and 6-benzyl-3-methyl-5,6,7,8-tetrahydro-1H-pyrido[4,3-d]pyrimidine-2,4-dione hydrochloride was precipitated with a solution of hydrochloric acid in ether, while cooling with ice. The product was purified by recrystallization from isopropanol.

WORKUP

后处理

  1. custom6-benzyl-3-methyl-5,6,7,8-tetrahydro-1H-pyrido[4,3-d]pyrimidine-2,4-dione hydrochloride was precipitated with a solution of hydrochloric acid in ether
  2. temperaturewhile cooling with ice
  3. customThe product was purified by recrystallization from isopropanol