HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 3-benzyl-5,6,7,8-tetrahydro-1H-pyrido[4,3-d]pyrimidine-2,4-dione hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 3-benzyl-5,6,7,8-tetrahydro-1H-pyrido[4,3-d]pyrimidine-2,4-dione | HCID 19423335 | — |
| Solvent | Water | HCID 962 | — |
| Product | 3-benzyl-5,6,7,8-tetrahydro-1H-pyrido[4,3-d]pyrimidine-2,4-dione hydrochloride | HCID 19423334 | — |
Reaction Steps
9.4 g of 3-benzyl-5,6,7,8-tetrahydro-1H-pyrido[4,3-d]-pyrimidine-2,4-dione were suspended in 250 ml of water, the equivalent amount of 1 N HCl was added and the solution formed was filtered and concentrated under vacuum. 9.9 g of 3-benzyl-5,6,7,8-tetrahydro-1H-pyrido[4,3-d]pyrimidine-2,4-dione hydrochloride were obtained from the residue after purification by recrystallization from isopropanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05556854 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-53f30d7e9842416aaa5eed1bc740ce8f |
| Source note | uspto-grants-1996_09 |