HRID742966

反应详情

EQUATION

反应方程式

HRID 742966 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

9.4 g of 3-benzyl-5,6,7,8-tetrahydro-1H-pyrido[4,3-d]-pyrimidine-2,4-dione were suspended in 250 ml of water, the equivalent amount of 1 N HCl was added and the solution formed was filtered and concentrated under vacuum. 9.9 g of 3-benzyl-5,6,7,8-tetrahydro-1H-pyrido[4,3-d]pyrimidine-2,4-dione hydrochloride were obtained from the residue after purification by recrystallization from isopropanol.

WORKUP

后处理

  1. customthe solution formed
  2. filtrationwas filtered
  3. concentrationconcentrated under vacuum