HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19423444, compound → HCID 19027729, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19423444 | HCID 19423444 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 19027729 | HCID 19027729 | 168.2% |
Reaction Steps
5-Acetylamino-1-{3-[4-(3-chlorophenyl)-1-piperazinyl]propyl}-3,4-dihydrocarbostyril (800 mg) was dissolved in 20 ml of 6 N hydrochloric acid, and the mixture was heated under reflux for 1 hour. The reaction mixture was concentrated under reduced pressure and the residue was recrystallized from ethanol to give 480 mg of 5-amino-1-{3-[4-(3-chlorophenyl)-1-piperazinyl]propyl}-3,4-dihydrocarbostyril dihydrochloride as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05556857 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-ad3b480fff13480c941b0c5c1944133d |
| Source note | uspto-grants-1996_09 |