HRID743010

反应详情

EQUATION

反应方程式

HRID 743010 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The product from Example 12c (78 g) was added to a solution of potassium hydroxide (50 g, 0.78 mol) in water (600 ml) and the mixture was refluxed overnight. After addition of activated carbon (2 g) and sodium sulfite (0.5 g) the mixture was allowed to cool, with stirring to room temperature and then filtered.

WORKUP

后处理

  1. temperaturethe mixture was refluxed overnight
  2. temperatureto cool
  3. filtrationfiltered