HuagongsheHuagongshe Chemistry Print Report · For research reference only
Epibromohydrin → HCID 19423887, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Epibromohydrin | HCID 18430 | — |
| Reactant | HCID 19423843 | HCID 19423843 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 19423887 | HCID 19423887 | 88% |
Reaction Steps
Following a procedure similar to that described in Example 1(a), 3.04 g of 2-[4-(4-isopropylphenyl)butyl]phenol (prepared as described in Preparation 8), 1.27 g of potassium t-butoxide and 3.11 g of epibromohydrin were reacted in 60 ml of dimethylacetamide. The crude product, extracted as described in Example 1(a), was purified as described in Example 1(a), to give 3.23 g (yield 88%) of the title compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05556864 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-66315b81c51b4d69bc09000132058052 |
| Source note | uspto-grants-1996_09 |