HuagongsheHuagongshe Chemistry Print Report · For research reference only
Epibromohydrin → HCID 19423936, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Epibromohydrin | HCID 18430 | — |
| Reactant | HCID 19423897 | HCID 19423897 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 19423936 | HCID 19423936 | 73% |
Reaction Steps
Following a procedure similar to that described in Example 1(a), 0.70 g of 2-[4-(4-methylphenyl)butyl]phenol (prepared as described in Preparation 6), 0.33 g of potassium t-butoxide and 0.8 g of epibromohydrin were reacted in 40 ml of dimethylacetamide. The crude product, extracted as described in Example 1(a), was purified as described in Example 1(a), to give 0.63 g (yield 73%) of the title compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05556864 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-4d55730a5d2c43dc898d34d2bb972c5a |
| Source note | uspto-grants-1996_09 |