HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 19423939, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | HCID 19424026 | HCID 19424026 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 19423939 | HCID 19423939 | 95% |
Reaction Steps
Following a procedure similar to that described in Example 1(b), 1.40 g of 2-{2-[4-(3-methoxymethoxyphenyl)butyl]phenoxymethyl]oxirane [prepared as described in step (a) above] dissolved in 14 ml of tetrahydrofuran were treated with 2.8 ml of 50% by volume aqueous dimethylamine. The crude product was purified as described in Example 1(b), to give 1.51 g (yield 95%) of the title compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05556864 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-03fcdf82af974687b4e15f6e71501765 |
| Source note | uspto-grants-1996_09 |