Hydrochloric Acid → HCID 19423874, compound

Participants

Reaction Steps

Following a procedure similar to that described in Example 1(c), 987 mg of 3-dimethylamino-1-[2-(3-methyl-4phenylbutyl)phenoxy]-2-propanol [prepared as described in step (b) above] dissolved in 20 ml of ethyl acetate were converted to the hydrochloride by treating it with 0.9 ml of a 4N solution of hydrogen chloride in dioxane. The solvent was then removed by distillation under reduced pressure, and the resulting residue was dried in vacuo, to give 1.09 g (a quantitative yield) of the title compound as a colorless oil.

Provenance & Evidence