HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2-(2-{2-[2-(3-Methoxyphenyl)ethyl]phenoxy}-ethyl]-1-methylpyrrolidine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2-(2-{2-[2-(3-Methoxyphenyl)ethyl]phenoxy}ethyl)-1-methylpyrrolidine | HCID 15896863 | — |
| Product | 2-(2-{2-[2-(3-Methoxyphenyl)ethyl]phenoxy}-ethyl]-1-methylpyrrolidine hydrochloride | HCID 19423854 | 36% |
Reaction Steps
Following a procedure similar to that described in Example 35(a), 5.70 g of 2-(2-{2-[2-(3-methoxyphenyl)ethyl]phenoxy}ethyl)-1-methylpyrrolidine [prepared as described in step (a) above] were converted to the hydrochloride, to give 4.89 g (yield 36%) of the title compound as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05556864 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-0da05a922f3d43e0866a0f01a6299495 |
| Source note | uspto-grants-1996_09 |