Hydrochloric Acid → HCID 19423839, compound

Participants

Reaction Steps

125 mg of 1-methyl-2-{2-[2-(5-phenylpentyl)phenoxy]ethyl}pyrrolidine [prepared as described in step (a) above] were dissolved in 3 ml of dioxane, and 0.13 ml of a 4N solution of hydrogen chloride in dioxane was added to the solution. The resulting mixture was then shaken and concentrated by distillation under reduced pressure. Pentane was added to the resulting concentrate, and the mixture was agitated and then concentrated by distillation under reduced pressure. This operation was repeated twice, and then he resulting oil was dried in vacuo, to give 0.138 g (a quantitative yield) of the title compound as a colorless oil.

Provenance & Evidence