HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-(naphthalen-2-yl)propanoate → 2-Naphthalenepropanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-(naphthalen-2-yl)propanoate | HCID 14022513 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 2-Naphthalenepropanol | HCID 11206232 | — |
Reaction Steps
Following a procedure similar to that described in the first part of Preparation 4, the whole of this ethyl 3-(2-naphthyl)propionate was reacted with 668 mg of lithium aluminum hydride in tetrahydrofuran at room temperature for 1.5 hours. At the end of this time, the reaction mixture was worked up and purified as described in the first part of Preparation 4, to give 3.29 g of 3-(2-naphthyl)propanol as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05556864 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-369aca6a51a94293a501737d7028e18b |
| Source note | uspto-grants-1996_09 |