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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 743404생성일: 2026년 10월 25일

1-(2-Benzyloxyphenyl)-4-(2-chlorophenyl)butadiene → 1-(2-Benzyloxyphenyl)-4-(2-chlorophenyl)butane

https://huagongshe.com/reaction/743404

반응식

참여 물질

역할이름HCID투입량
반응물1-(2-Benzyloxyphenyl)-4-(2-chlorophenyl)butadieneHCID 53895274—
용매EthanolHCID 702—
용매TetrahydrofuranHCID 8028—
생성물1-(2-Benzyloxyphenyl)-4-(2-chlorophenyl)butaneHCID 1942401862.4%

반응 단계

Following a procedure similar to that described in the latter part of Preparation 3, 4.53 g of this 1-(2-benzyloxyphenyl)-4-(2-chlorophenyl)butadiene were dissolved in a 4:1 by volume mixture of tetrahydrofuran and ethanol and were hydrogenated, whilst ice-cooling. The reaction mixture was then worked up as described in the latter part of Preparation 3, to give 2.86 g (yield 62%) of 1-(2-benzyloxyphenyl)-4-(2-chlorophenyl)butane.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05556864
출처 데이터셋uspto-grants-1996_09
ORD IDord-40e3be322e02424ea21c8208c349c5df
출처 메모uspto-grants-1996_09