HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromoacetyl bromide → Bromoacetyl-5-amino-1,10-phenanthroline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromoacetyl bromide | HCID 61147 | — |
| Reactant | 1,10-Phenanthrolin-5-amine | HCID 606970 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | Bromoacetyl-5-amino-1,10-phenanthroline | HCID 19424582 | — |
Reaction Steps
5-Amino-1,10-phenanthroline (2) (Preparation 1; 1.28 g; 6.54 mmol) was dissolved with heating in 200 ml anhydrous acetonitrile. Into this solution, was added bromoacetyl bromide (Aldrich; 6.60 g; 32.7 mmol) in 7.2 ml anhydrous acetonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05556949 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-3a5d35ea945b4913a7bc2bf9ce07d65b |
| Source note | uspto-grants-1996_09 |