反应详情

5-Amino-1,10-phenanthroline (2) (Preparation 1; 1.28 g; 6.54 mmol) was dissolved with heating in 200 ml anhydrous acetonitrile. Into this solution, was added bromoacetyl bromide (Aldrich; 6.60 g; 32.7 mmol) in 7.2 ml anhydrous acetonitrile.