HCID 178473533, compound → HCID 178512138, compound

HRID 744042Notes

Reaction equation

HRID 744042 reaction equation
C(OC([NH:6][C:7]([NH:16][CH2:17][CH2:18][CH2:19][C:20]1[N:21]=[CH:22][NH:23][CH:24]=1)=[N:8][CH2:9][CH:10]1[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11]1)=O)C>Cl>[NH:23]1[CH:24]=[C:20]([CH2:19][CH2:18][CH2:17][NH:16][C:7]([NH:8][CH2:9][CH:10]2[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15]2)=[NH:6])[N:21]=[CH:22]1

Participants

3

Reactant 1

HCID 178473533HCID 178473533, compound

Product 1

HCID 178512138HCID 178512138, compound

Reagents, catalysts & solvents 1

HCID 313Hydrochloric AcidSolvent

Procedure

1.5 mmol of the compound obtained in Example 52 are brought to reflux for 30 min in 15 ml of 1N hydrochloric acid and are then concentrated to dryness. The residual dry form is crystallized from diethyl ether.

Workup

  1. concentrationare then concentrated to dryness
  2. customThe residual dry form is crystallized from diethyl ether

Sources & evidence

ORD record
ord-ec7e9c0dc0a14e4caf5277b87afb8141
Source dataset
uspto-grants-1996_09
Patent number
US05559113

Reaction notes

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