HCID 19696535, compound → 157023-27-3

Participants

Reaction Steps

A solution of 1-3 (1.70 g, 4.13 mmol) in THF (80 ml) was cooled to -78° and treated with n-BuLi (4.25 mmol) with stirring for 15 min. The reaction was then quenched with 10% KHSO4 (25 ml) and the solvent was removed. The residue was taken up in Et2O (150 ml) and this was washed with 10% KHSO4 solution, brine, and dried (Na2SO4).

Provenance & Evidence