HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Pyridinepropanol → HCID 19696542, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Pyridinepropanol | HCID 72923 | — |
| Reactant | Acetic acid ethanol water | HCID 86584229 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 19696542 | HCID 19696542 | — |
Reaction Steps
Commercially available 4-pyridinepropanol (6-10) (38 g, 277 mmol) was dissolved in 100 ml EtOH/HOAc/H2O (4:1:1) and treated with 2.0 g 10% Pd/C. This mixture was hydrogenated on a Parr reactor for 24 h at 55 psi. The catalyst was removed by filtration and the filtrate evaporated to give 3-(4-piperidinyl)propyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05559127 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-d9ba7946cc334b3fbcc21ae753eadec4 |
| Source note | uspto-grants-1996_09 |