HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 67770761, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 54134198 | HCID 54134198 | — |
| Product | HCID 67770761 | HCID 67770761 | 95.7% |
Reaction Steps
The operation is carried out as in Example 2 starting with 28.6 g of the product obtained in Example 11, using 3.3 g sodium hydride. 24.74 g of desired product is obtained which is used as it is for the following example. M.p.=110°-115° C. crystallized from diethyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05559130 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-a1dad9e03bce443daa18a7c5bd59ed08 |
| Source note | uspto-grants-1996_09 |