HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22865603, compound → HCID 22865605, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22865603 | HCID 22865603 | — |
| Solvent | Ammonia methanol | HCID 21705897 | — |
| Product | HCID 22865605 | HCID 22865605 | 67.1% |
Reaction Steps
Compound 19 (0.61 g, 1.06 mmol) in NH3 /MeOH (40 ml) was stirred at room temperature overnight. The solvent was evaporated and the residue was purified on preparative plates using MeOH/CHCl3 (20%) to give pure compound 21 (0.185 g, 66.5%) as yellow foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05559101 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-c1e4977edfe74a30a42db295c76b526e |
| Source note | uspto-grants-1996_09 |