HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 744645Generated: October 30, 2026
Diethylene Glycol Monomethyl Ether → HCID 19075261, compound
https://huagongshe.com/reaction/744645
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diethylene Glycol Monomethyl Ether | HCID 8134 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 3-Chloro-4-(pyridin-3-yl)-1,2,5-thiadiazole | HCID 10488164 | — |
| Product | HCID 19075261 | HCID 19075261 | — |
Reaction Steps
To a solution of sodium (210 mg, 9 mmol) in 2-(2-methoxyethoxy)ethanol (10 ml) was added 3-(4-chloro-1,2,5-thiadiazol-3-yl)pyridine (590 mg, 3 mmol). The mixture was stirred at 50° C. for 4 h and evaporated. The residue was dissolved in water and extracted with ether. The combined organic phases were dried and evaporated to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05559138 |
|---|
| Source dataset | uspto-grants-1996_09 |
|---|
| ORD ID | ord-88b082b864ff48b58b9d07b8bbe3091d |
|---|
| Source note | uspto-grants-1996_09 |
|---|
