HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropyl chloroformate → Methylenechloride Hexane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropyl chloroformate | HCID 7917 | — |
| Reactant | Isovaleryl chloride | HCID 66054 | — |
| Product | Methylenechloride Hexane | HCID 21226440 | 87% |
Reaction Steps
This compound was prepared according to the method described in Example 7, except that isopropyl chloroformate was replaced by an equivalent portion of isovaleryl chloride. The product was purified by recrystallization from a mixture of hexane/dichloromethane as colourless crystals mp 97°-80° C., yield 87%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05559145 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-a0d03c1e0287463995d930e90d703661 |
| Source note | uspto-grants-1996_09 |