HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropyl chloroformate → Methylenechloride Hexane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropyl chloroformate | HCID 7917 | — |
| Reactant | 2-Fluorobenzoyl chloride | HCID 9808 | — |
| Product | Methylenechloride Hexane | HCID 21226440 | 81% |
Reaction Steps
This compound was prepared according to the method described in Example 7, except that isopropyl chloroformate was replaced by an equivalent portion of o-fluorobenzoyl chloride and the reaction product was purified by recrystallization from a mixture of hexane/dichloromethane as colourless crystals mp 113.5°-114° C., yield 81%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05559145 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-efb98f5da6b5460b8e082c46d6aa1632 |
| Source note | uspto-grants-1996_09 |