HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19422046, compound → HCID 19422048, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19422046 | HCID 19422046 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Tetrachloroethylene | HCID 31373 | — |
| Product | HCID 19422048 | HCID 19422048 | — |
Reaction Steps
The mixture of 27,5 g of 1-benzyl-5-(1-hydroxy-4-phenylbutyl)-1H-imidazole and 34,4 g of manganese dioxide in 550 ml of tetrachloroethylene is refluxed stirring for four hours. The reaction mixture is filtered and the filtrate is evaporated to dryness. The product is crystallized from ethyl acetate as hydrochloride salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05559141 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-748f8fe0c3bc4ab7b044672bbd60e757 |
| Source note | uspto-grants-1996_09 |