HCID 6915783, compound → HCID 74972732, compound

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Reaction Steps

Starting from N-Boc-L-cyclohexylalanine in place of N-Boc-L-phenylalanine, the title Compound 14 (white solid) was prepared using procedures analogous to those described for Compounds 1b(i), 4b, and 7. [α]D =-33.7° (c 0.18, MeOH). 13C NMR (CDCl3): δ26.1, 26.4, 26.5, 28.4, 32.3, 34.2, 34.3, 38.1, 51.0, 51.6, 72.7, 79.5, 156.4. Mass Spec. (M+H )+ @556. High Resolution FAB; exact mass calcd. for C30H58O6N3 (M+H)+, 556,4325; Found 556.4304.

Provenance & Evidence