HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 49823212, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 6915783 | HCID 6915783 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 49823212 | HCID 49823212 | — |
Reaction Steps
A mixture of Compounds 26a(i) and 26a(ii) were reacted with Compound 27a by a procedure analogous to that used for the preparation of Compound 4b (except that MeOH at 55° was used in place of DMF) to give the title Compound 27b as a mixture of diastereomers. m.p. 156°-159° C.; MS: (CI/NH3): 544 (M+H). Anal. Calc. for C30H45N3O6 ·0.16 H2O
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05559256 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-1b6fddeb79724d34af69831bd4620a47 |
| Source note | uspto-grants-1996_09 |