Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 745123Generated: November 1, 2026

Methanol → HCID 49823212, compound

https://huagongshe.com/reaction/745123

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantHCID 6915783HCID 6915783—
SolventDimethylformamideHCID 6228—
ProductHCID 49823212HCID 49823212—

Reaction Steps

A mixture of Compounds 26a(i) and 26a(ii) were reacted with Compound 27a by a procedure analogous to that used for the preparation of Compound 4b (except that MeOH at 55° was used in place of DMF) to give the title Compound 27b as a mixture of diastereomers. m.p. 156°-159° C.; MS: (CI/NH3): 544 (M+H). Anal. Calc. for C30H45N3O6 ·0.16 H2O

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05559256
Source datasetuspto-grants-1996_09
ORD IDord-1b6fddeb79724d34af69831bd4620a47
Source noteuspto-grants-1996_09